32228-99-2
- Product Name：N-Phenyl-4-biphenylamin
- Molecular Formula：C18H15N
- Purity：99%
- Molecular Weight：245.324
Product Details;
CasNo： 32228-99-2
Molecular Formula： C18H15N
Buy High Quality 99% Pure N-Phenyl-4-biphenylamin 32228-99-2 Safe Shipping
- Molecular Formula:C18H15N
- Molecular Weight:245.324
- Vapor Pressure:5.68E-07mmHg at 25°C
- Melting Point:113 °C
- Refractive Index:1.646
- Boiling Point:411.2 °C at 760 mmHg
- PKA:0.73±0.20(Predicted)
- Flash Point:217.6 °C
- PSA：12.03000
- Density:1.111 g/cm3
- LogP:5.17020
N-Phenyl-4-biphenylamine(Cas 32228-99-2) Usage
|
Uses |
N-Phenyl-4-biphenylamine (cas# 32228-99-2) is a useful reagent for the preparation of heterocyclic compounds for organic electrical devices. |
InChI:InChI=1/C18H15N/c1-3-7-15(8-4-1)16-11-13-18(14-12-16)19-17-9-5-2-6-10-17/h1-14,19H
32228-99-2 Relevant articles
Organic compound and electronic device and device containing the same
-
Paragraph 0230; 0257-0259, (2021/09/11)
The invention relates to the technical f...
Organic compound, electronic device comprising organic compound and electronic equipment
-
Paragraph 0116-0118, (2021/08/07)
The invention relates to an organic comp...
Organic compound and electronic component and electronic device comprising same
-
Paragraph 0113-0115, (2021/07/17)
The invention provides an organic compou...
Organic compound, and electronic element and electronic device using same
-
Paragraph 0150-0151, (2021/07/14)
The invention relates to an organic comp...
32228-99-2 Process route
-
-
108-86-1,52753-63-6
bromobenzene
-
-
92-67-1
4-phenylalanine
-
-
32228-99-2
4-phenyldiphenylamine
| Conditions | Yield |
|---|---|
|
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos;
In
toluene;
at 108 ℃;
for 2h;
Inert atmosphere;
|
86% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos;
In
toluene;
at 108 ℃;
for 2h;
Inert atmosphere;
|
86% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
at 80 ℃;
|
75% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos;
In
toluene;
for 1h;
Inert atmosphere;
Reflux;
|
75% |
|
With
tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate;
In
toluene;
at 110 ℃;
Inert atmosphere;
|
73% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
for 5h;
Inert atmosphere;
Reflux;
|
65% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate;
In
toluene;
at 100 ℃;
for 7h;
Inert atmosphere;
|
65% |
|
With
potassium phosphate; XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
toluene;
for 20h;
Heating;
|
-
-
62-53-3
aniline
-
-
2051-62-9,80333-62-6
4'-biphenyl chloride
-
-
32228-99-2
4-phenyldiphenylamine
| Conditions | Yield |
|---|---|
|
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos;
In
toluene;
at 70 ℃;
for 1h;
Inert atmosphere;
|
89.3% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos;
In
toluene;
at 65 - 75 ℃;
for 1h;
Inert atmosphere;
|
86.9% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos;
In
toluene;
at 20 - 70 ℃;
for 1h;
Inert atmosphere;
|
86.9% |
|
aniline; 4'-biphenyl chloride;
With
palladium diacetate; sodium sulfate; sodium t-butanolate; XPhos;
for 1h;
Milling;
In
water; ethyl acetate;
for 0.0333333h;
Milling;
|
62% |
|
With
[tert-butyloxy]bis(N,N-diisopropylamino)phosphane; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate;
In
toluene;
at 105 ℃;
for 24h;
Inert atmosphere;
Schlenk technique;
|
32228-99-2 Upstream products
-
101895-15-2
2-[(4-biphenyl)amino]benzoic acid
-
92-66-0
4-bromo-1,1'-biphenyl
-
103-84-4
Acetanilid
-
92-52-4
biphenyl
32228-99-2 Downstream products
-
4018-68-2
3-phenyl-10H-phenothiazine
-
101716-47-6
biphenyl-4-yl-nitroso-phenyl-amine
-
103012-26-6
3-phenyl-9H-carbazole
-
938469-97-7
C55H40N4O
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